Refine
Document Type
- Article (3)
- Part of Periodical (1)
Language
- English (4)
Is part of the Bibliography
- yes (4)
Keywords
- FIB-SEM tomography (1)
- FeNiCrAl (1)
- Materialermüdung (1)
- nitridation (1)
- void formation (1)
Institute
- Fakultät IuI (4)
The present study gives an overview of recent investigations dealing with the fatigue behaviour of the tempered martensitic steel 50CrMo4 (Fe-0.5wt%C-1wt%Cr) in the HCF and VHCF regime by taking into account a variation in material strength, by modifying the heat treatment parameters. The parameters for the tempering treatment were adapted to receive two material conditions with 37HRC and 57HRC, respectively. Subsequently, fatigue specimens were machined from the heat-treated bars for fatigue tests in an ultrasonic (f=20000Hz) and a resonance (f=95Hz) fatigue testing machine under fully reversed loading (R=-1) at laboratory air atmosphere. It was found that the dominant fatigue and fracture mechanisms change with increasing material strength. For 37HRC moderate-strength specimens crack initiation was shown to occur on the specimen surface within Cr depleted bands (segregation bands) as the dominant fatigue damage mechanism. Contrary to that, only internal crack initiation at non-metallic inclusions was observed for the high strength 57HRC condition. Furthermore, the completely different crack initiation mechanisms of the two heat treatment conditions were assessed by applying the Murakami approach relating the fatigue limit with the size of non-metallic inclusions.
A recently published study of high temperature nitridation of iron chromium aluminum alloys (FeCrAl) at 900°C in N2–H2 has redundantly shown the formation of locally confined corrosion pockets reaching several microns into the alloy. These nitrided pockets form underneath chromia islands laterally surrounded by the otherwise protective alumina scale. Chromia renders a nitrogen‐permeable defect under the given conditions and the presence of aluminum in the alloy. In light of these findings on FeCrAl, a focused ion beam–scanning electron microscope tomography study has been undertaken on an equally nitrided FeNiCrAl sample to characterize its nitridation corrosion features chemically and morphologically. The alloy is strengthened by a high number of chromium carbide precipitates, which are also preferential chromia formation sites. Besides the confirmation of the complete encapsulation of the corrosion pocket from the alloy by a closed and dense aluminum nitride rim, very large voids have been found in the said pockets. Furthermore, metallic particles comprising nickel and iron are deposited on top of the outer oxide scale above such void regions.
In this experimental work, the quasi static and fatigue properties of a 40 wt.% long carbon fiber reinforced partially aromatic polyamide (Grivory GCL-4H) were investigated. For this purpose, microstructural parameter variations in the form of different thicknesses and different removal directions from injectionmolded plates were evaluated. Mechanical properties decreased by increasing misalignment away from the melt flow direction. By changing the specimen thickness, no change in the general fiber distribution pattern transversal and normal to the axis of melt flow was observed. It has shown that with increasing specimen thickness the quasi static properties along the melt flow direction decreased and vice versa resulting in superior properties normal to the melt flow axis. At around 5 mm, an intersection suggests quasi-isotropic behavior. In addition, the fatigue strength of the material was significantly higher in the flow direction than normal to the flow direction. No change in fatigue life was observed while changing specimen thickness. The Basquin equation seems to describe the effect of stress amplitude on the fatigue strength of this composite. Scanning electron microscopy was used to investigate fracture surfaces of tested specimens. Results show that mechanical properties and morphological structures depend highly on fiber orientation.